Inorganic Syntheses, Volume 7

Copyright © 1963 by the McGraw-Hill Book Company, Inc.

Inorganic Syntheses, Volume 7

Editor(s): Jacob Kleinberg

Published Online: 5 JAN 2007

Print ISBN: 9780470131664

Online ISBN: 9780470132388

DOI: 10.1002/9780470132388

About this Book

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About The Product

The volumes in this continuing series provide a compilation of current techniques and ideas in inorganic synthetic chemistry. Includes inorganic polymer syntheses and preparation of important inorganic solids, syntheses used in the development of pharmacologically active inorganic compounds, small-molecule coordination complexes, and related compounds. Also contains valuable information on transition organometallic compounds including species with metal-metal cluster molecules. All syntheses presented here have been tested.

Table of contents

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      Frontmatter (pages i–xi)

  2. Part IA: CHAPTER IA

    1. Lithium Hydroxide and Lithium Oxide (pages 1–5)

      Justo Bravo and Johan H. De Groot

  3. Part IB: CHAPTER IB

    1. 1-Phenylbiguanide-p-sulfonic Acid Complexes of Copper(II) (pages 6–8)

      Priyadaranjan Rây, Sam N. Holter and W. Conard Fernelius

    2. Tetrakis[iodo(tri-n-butylphosphine)copper(I)] and Iodo-(2,2′-Bipyridine)-(Tri-n-butylphosphine)copper(I) (pages 9–12)

      George B. Kauffman, Larry A. Teter, T. C. Ichniowski and A. F. Clifford

  4. Part IIA: CHAPTER IIA

    1. Barium Iodate 1-Hydrate (pages 13–15)

      Jack L. Lambert, Stanley K. Yasuda and H. Schauble

  5. Part IIIA: CHAPTER IIIA

    1. Gallium (III) Nitride (pages 16–18)

      Richard C. Schoonmaker, Claudia E. Burton, J. Lundstrom and J. L. Margrave

    2. Indium(I) Bromide (pages 18–21)

      R. J. Clark, Ernest Griswold, Jacob Kleinberg, Richard D. Barnes and John D. Corbett

  6. Part IVA: CHAPTER IVA

    1. Hexachlorodisiloxane (pages 22–28)

      B. A. Grigor, C. J. Wilkins, A. T. Brault and R. J. Angelici

    2. Trichlorosilanethiol (pages 28–30)

      D. J. Panckhurst, C. J. Wilkins, A. T. Brault and R. J. Angelici

    3. Tris(acetylacetonato)silicon Chloride Hydrochloride and Some Derivatives (pages 30–34)

      Reed F. Riley, Robert West, Robert Barbarin, George Slusarczuk and Stanley Kirschner

    4. Hydrides of Germanium, Tin, Arsenic, and Antimony (pages 34–44)

      William L. Jolly, John E. Drake, Ralph Rudolph and T. Wartik

  7. Part IVB: CHAPTER IVB

    1. Titanium(III) Chloride (pages 45–50)

      W. L. Groeneveld, G. P. M. Leger, J. Wolters, R. Waterman and A. L. Mcclelland

    2. Bis[tris(acetylacetonato)titanium(IV)] Hexachlorotitanate(IV) (pages 50–51)

      Vera Doron and Duward Shriver

    3. Zirconium(IV) Iodide (pages 52–54)

      Kenneth C. Eberly and Bert Chamberland

  8. Part VA: CHAPTER VA

    1. Biguanide Sulfate (pages 55–58)

      D. Karipides, W. Conard Fernelius and Melvin D. Joeston

    2. Biguanide (pages 58–59)

      Samuel N. Holter, W. Conard Fernelius and Devon Meek

    3. Black Phosphorus (pages 60–62)

      H. Krebs and H. Majewski

    4. Pentacalcium Monohydroxyorthophosphate (pages 63–65)

      Erich Hayek, Heinrich Newesely and Max L. Rumpel

    5. Tetraammonium Pyrophosphate (pages 65–67)

      C. Swanson, F. Mccollough and Ralph K. Birdwhistell

    6. (Triphenyl)aminophosphonium Chloride (pages 67–69)

      Harry H. Sisler, Nathan L. Smith and Peter Barna

    7. (Dimethylamido)phosphoryl Dichloride (pages 69–71)

      E. N. Walsh, A. D. F. Toy, M. L. Nielsen and T. J. Morrow

    8. Bis(dimethylamido)phosphoryl Chloride (pages 71–73)

      E. N. Walsh, A. D. F. Toy, M. L. Nielsen and T. J. Morrow

    9. Octamethylpyrophosphoramide (pages 73–76)

      A. D. F. Toy, E. N. Walsh, M. L. Nielsen and T. J. Morrow

    10. Trimeric and Tetrameric Phosphonitrile Bromides (pages 76–79)

      Karl John, Therald Moeller, Raymond E. Mcglothlin and R. A. Zingaro

    11. Phosphorus(V) Chloride-Boron Chloride Complex (pages 79–81)

      R. R. Holmes and H. Majewski

    12. Phosphorus(V) Chloride-Gallium(III) Chloride Complex (pages 81–82)

      R. R. Holmes, R. N. Ramsey and John D. Corbett

    13. Methylbromoarsines (pages 82–86)

      Ludwig Maier and William Jensen

  9. Part VB: CHAPTER VB

    1. Vanadium(III) Fluoride (pages 87–92)

      B. J. Sturm, C. W. Sheridan, P. H. Crayton and R. N. Vance

    2. Vanadium(III) Sulfate (pages 92–94)

      Robert T. Claunch, Mark M. Jones and Wayne C. Wolsey

    3. Vanadium(II) Sulfate (pages 94–96)

      Maksymilian Kranz, David E. Goldberg and Aaron Ribner

    4. Vanadium(II) Hydroxide (pages 97–99)

      Maksymilian Kranz, David E. Goldberg and Aaron Ribner

    5. Cyclopentadienyl Metal Carbonyls and Some Derivatives (pages 99–115)

      R. B. King, F. G. A. Stone, William L. Jolly, Gordon Austin, William Covey, David Rabinovich, Henry Steinberg and Roy Tsugawa

  10. Part VIA: CHAPTER VIA

    1. Sulfur(S35 (pages 116–119)

      C. Briske, N. H. Hartshorne, D. R. Stranks and Floyd B. Baker

    2. Sulfur(IV) Fluoride (pages 119–124)

      F. S. Fawcett, C. W. Tullock and Claude I. Merrill

    3. Peroxydisulfuryl Difluoride (pages 124–128)

      Jean' Ne M. Shreeve, George H. Cady, Charles Cleaver and E. L. Muetterties

    4. Sodium Hydrogen Sulfide (pages 128–131)

      Richard E. Eibeck, Ralph A. Zingaro and Raymond E. Mcglothlin

  11. Part VIB: CHAPTER VIB

    1. Trichloro(tripyridine)chromium(III) (pages 132–134)

      James C. Taft, Mark M. Jones, Ronald S. Schreiber and Henry F. Holtzclaw

    2. Tris(3-bromoacetylacetonato)chromium(III) (pages 134–136)

      James P. Collman, George B. Kauffman and Stanley E. Gordon

    3. Cyclopentadienyl Tricarbonyl Hydrides of Chromium, Molybdenum, and Tungsten [Hydrogen Tricarbonyl(Cyclopentadienyl)Chromate(0), -Molybdate(0), and -Tungstate(0)] (pages 136–139)

      E. O. Fischer and Roy L. Pruett

    4. Trichloro(tripyridine)molybdenum(III) (pages 140–142)

      Hans B. Jonassen, Lionel J. Bailin, George Slusarczuk and Stanley Kirschner

    5. Potassium Octacyanotungstate(IV) 2-Hydrate (pages 142–146)

      Edward A. Heintz and Wilmer J. Stratton

    6. Uranyl Chloride 1-Hydrate (pages 146–148)

      Jack D. Hefley, Daniel M. Mathews, Edward S. Amis, I. Sheft and Joseph J. Katz

  12. Part VIIA: CHAPTER VIIA

    1. Sodium Fluoride(F18) (pages 149–154)

      D. R. Stranks and Floyd B. Baker

    2. Chlorine(Cl36)-Labeled Deuterium Chloride: [Hydrogen-D Chloride (Cl36)] (pages 155–160)

      R. H. Herber and B. J. Masters

    3. Chlorine(Cl36)-Labeled Thionyl Chloride, Silicon Tetrachloride, Boron Chloride, Germanium(IV) Chloride, and Phosphorus(III) Chloride (pages 160–162)

      R. H. Herber and Floyd B. Baker

    4. Anhydrous Metal Chlorides (pages 163–169)

      E. R. Epperson, S. M. Horner, K. Knox, S. Y. Tyree, J. R. Crook and George Gibson

    5. Unipositive Halogen Complexes (pages 169–176)

    6. Monopyridineiodine(I) Chloride (pages 176–180)

      George B. Kauffman, Kenneth L. Stevens and Donald J. Royer

    7. Anhydrous Hydrogen Iodide (pages 180–182)

      C. J. Hoffman and Edward A. Heintz

  13. Part VIIB: CHAPTER VIIB

    1. Acetylacetonato manganese(III) (pages 183–184)

      Robert G. Charles and B. E. Bryant

    2. Rhenium(III) Iodide (pages 185–189)

      L. Malatesta, Colin Lock and Geoffrey Wilkinson

    3. Potassium Hexachlororhenate(IV) and Potassium Hexabromorhenate(IV) (pages 189–192)

      George W. Watt, Richard J. Thompson and Jean M. Gibbons

  14. Part VIII: CHAPTER VIII

    1. Triiron Dodecacarbonyl (pages 193–196)

      R. B. King, F. G. A. Stone, R. S. Summitt and W. E. Edgell

    2. Sodium Salts of Carbonyl Hydrides Prepared in Ethereal Media (pages 196–201)

      R. B. King and F. G. A. Stone

    3. Iron-Labeled Cyclopentadienyl Iron Complexes (pages 201–205)

      D. R. Stranks and Floyd B. Baker

    4. Tris(3-nitroacetylacetonato)cobalt(III) (pages 205–207)

      James P. Collman, William L. Young, George B. Kauffman and Michael F. Citro

    5. Inner Complexes of Cobalt(III) with Diethylenetriamine (pages 207–213)

      Philip H. Crayton, Fred Zitomer and Jack Lambert

    6. Hydrated Rhodium(III) Chloride, Chloroamminerhodium (III) Salts, and a Note on the Recovery of Rhodium Wastes (pages 214–220)

      Susan N. Anderson, Fred Basolo and E. I. Onstott

    7. cis- and trans-Tetrachloro(dipyridine)iridium(IV) (pages 220–224)

      George B. Kauffman, J. W. Hogarth and F. P. Dwyer

    8. cis- and trans-Trichlorotris(diethyl sulfide)iridium(III) (pages 224–228)

      George B. Kauffman, J. W. Hogarth and F. P. Dwyer

    9. cis- and trans-Pyridinium Tetrachloro(dipyridine)iridate(III) (pages 228–231)

      George B. Kauffman, J. W. Hogarth and F. P. Dwyer

    10. Recovery of Platinum from Laboratory Residues (pages 232–236)

      George B. Kauffman, Larry A. Teter and Richard N. Rhoda

    11. cis- and trans-Tetrachlorodiammineplatinum(IV) (pages 236–238)

      George B. Kauffman, George Slusarczuk and Stanley Kirschner

    12. cis- and trans-Dichlorodiammineplatinum(II) (pages 239–245)

      George B. Kauffman, Dwaine O. Cowan, George Slusarczuk and Stanley Kirschner

    13. cis- and trans-Dichlorobis(tri-n-butylphosphine)platinum(II) (pages 245–249)

      George B. Kauffman, Larry A. Teter and James E. Huheey

    14. cis- and trans-Dichloro(dipyridine)platinum(II) (pages 249–253)

      George B. Kauffman and Richard J. Thompson

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      Index of Contributers (pages 255–265)

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      Subject Index (pages 267–309)

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      Formula Index (pages 311–335)

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