Inorganic Syntheses, Volume 9

Inorganic Syntheses, Volume 9

Editor(s): S. Y. Tyree

Published Online: 5 JAN 2007

Print ISBN: 9780470131688

Online ISBN: 9780470132401

DOI: 10.1002/9780470132401

About this Book

The volumes in this continuing series provide a compilation of current techniques and ideas in inorganic synthetic chemistry. Includes inorganic polymer syntheses and preparation of important inorganic solids, syntheses used in the development of pharmacologically active inorganic compounds, small-molecule coordination complexes, and related compounds. Also contains valuable information on transition organometallic compounds including species with metal-metal cluster molecules. All syntheses presented here have been tested.

Table of contents

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  1. Part I: CHAPTER I

  2. Part II: CHAPTER II

    1. Dichlorobis(hydroxylamine)zinc(II) (Crismer's Salt) (pages 2–3)

      John E. Walker, David M. Howell, Richard J. Thompson and Billy C. Archibld


    1. Aluminum Derivative of Ethyl Acetoacetate (pages 25–27)

      R. G. Charles, N. C. Peterson, G. H. Franke, R. Steffl and E. M. Larsen

    2. Uranium(IV) Acetate (pages 41–43)

      R. C. Paul, J. S. Ghetra, M. S. Bains and Henry R. Hoekstra

  4. Part IV: CHAPTER IV

    1. Titanium(IV) Bromide (pages 46–50)

      Rolf B. Johannesen, Charles L. Gordon, Karl H. Gayer and Lawrence Balash

    2. Tetrakis(1,1,1-trifluoro-2,4-pentanedionato)zirconium(and Hafnium) (pages 50–52)

      Melvin L. Morris, Ross W. Moshier, Robert E. Sievers, Dean F. Martin, James E. Gano and Richard R. Woehrle

    3. Diphenylbis(1-phenyl-1,3-butanedionato)tin(IV) (pages 52–55)

      Wilfared H. Nelson, William J. Randall, Dean F. Martin, Gerald H. Reifenberg and William J. Considine

  5. Part V: CHAPTER V

    1. Phosphine (pages 56–58)

      Sudarshan D. Gokhale, William L. Jolly, Sherman Thomas and Doyle Britton

    2. Trimethylphosphine (pages 59–63)

      R. Thomas, Klaas Eriks, R. R. Holmes, R. P. Carter and E. Lanpher

    3. Phenyldibromophosphine (pages 73–75)

      Piero Nannelli, Gerald R. Feistel, Therald Moeller, C. P. Haber and A. J. Bilbo

    4. Vandium(V) Oxide (pages 80–83)

      Bertold Reuter, Jorg Jaskowsky, Robert E. Mccarley and John L. Meyer

    5. Vanadium(V) Oxide Nitrate and Chromium(VI) Oxide Nitrate (pages 83–88)

      Arlo D. Harris, John C. Trebellas, Hans B. Jonassen, Donald F. Clemens, Stephen Frazier and Harry H. Sisler

    6. Trimethylantimony Dihalides (pages 92–97)

      G. O. Doak, G. G. Long, M. E. Key, Lee W. Bush, David W. Thompson and A. L. Allred

  6. Part VI: CHAPTER VI

    1. Tetrasulfur Tetranitride, S4N4 (pages 98–102)

      Milagros Villena-Blanco, William L. Jolly, B. Zane Egan and Ralph A. Zingaro

    2. Sulfur Nitrogen Chlorides (pages 102–111)

      William L. Jolly, Keith D. Maguire, Dean F. Martin, James E. Gano, Richard Woehrle and Calvin Yoshida

    3. Cobalt(II) Sulfoxylate (pages 116–117)

      David T. Farrar, Mark M. Jones, Burl E. Bryant, Norman Dittrick and Thomas Grow

    4. Cycloheptatrienemolybdenum(0) Tricarbonyl (pages 121–122)

      F. A. Cotton, J. A. Mccleverty, J. E. White, R. B. King, A. F. Fronzaglia and M. B. Bisnette

    5. Tungsten Oxide Tetrachloride (pages 123–126)

      Susan E. Feil, S. Y. Tyree, F. N. Collier, Robert E. Mccarley and Peter B. Fleming


    1. Anhydrous Metal Chlorides (pages 133–136)

      W. W. Porterfield, S. Y. Tyree, Dean F. Martin and James R. Cook

    2. Tetrahalo Complexes of Dipositive Metals in the First Transition Series (pages 136–142)

      Naida S. Gill, F. B. Taylor, W. E. Hatfield, W. E. Parker, Carol S. Fountain and Fred L. Bunger

    3. Triorthoperiodatotetracobaltic(III) Acid (pages 142–144)

      Jack. M. Williams, C.J. Nyman, Adrienne E. Wickenden and Ronalds A. Krause

    4. Complexes of Rhenium(V) (pages 145–148)

      N. P. Johnson, C. J. L. Lock, G. Wilkinson, James L. Booker and Richard J. Thompson

    5. Trimethylsilyl Perrhenate (pages 149–151)

      Max Schmidt, Hubert Schmidbaur, Sherman Thomas and Doyle Britton


    1. Hexaamminecobalt(II) Chloride (pages 157–160)

      George B. Kauffman, Nobuyuki Sugisaka, Kenneth Emerson, Leo A. Bares and Clifford C. Houk

    2. Chloropentaamminecobalt(III) Chloride (pages 160–163)

      Gert G. Schlessinger, Doyle Britton, Thornton Rhodes and Elizabeth Ng

    3. Salts of Dinitrodiglycinatocobaltate(III) (pages 173–175)

      M. B. Celap, T. J. Janjic, D. J. Radanovic, Burl E. Bryant, L. Hern, R. Hatch and D. Sparkman

    4. Perchloratonickel(II) Complexes (pages 178–180)

      William E. Bull, L. E. Moore, L. M. Vallerino, Gene Hill and J. V. Quagliano

    5. Tetrakis(Triphenylphosphite)Nickel(0) (pages 181–182)

      J. R. Olechowski, C. G. Mcalister, R. F. Clark, L. J. Todd and S. A. Buell

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