Inorganic Syntheses, Volume 14

Copyright © 1973 by McGraw-Hill, Inc.

Inorganic Syntheses, Volume 14

Editor(s): Aaron Wold, John K. Ruff

Published Online: 5 JAN 2007

Print ISBN: 9780470131749

Online ISBN: 9780470132456

DOI: 10.1002/9780470132456

About this Book

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About The Product

The volumes in this continuing series provide a compilation of current techniques and ideas in inorganic synthetic chemistry. Includes inorganic polymer syntheses and preparation of important inorganic solids, syntheses used in the development of pharmacologically active inorganic compounds, small-molecule coordination complexes, and related compounds. Also contains valuable information on transition organometallic compounds including species with metal-metal cluster molecules. All syntheses presented here have been tested.

Table of contents

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      Frontmatter (pages i–xiv)

  2. Part I: Chapter one PHOSPHORUS COMPOUNDS

    1. Phosphine (pages 1–4)

      Robert C. Marriott, Jerome D. Odom, Curtis T. Sears, V. D. Bianco and S. Doronzo

    2. Tert-butyldichlorophosphine and Di-tert-butylchlorophosphine (pages 4–9)

      M. Fild, O. Stelzer, R. Schmutzler and G. O. Doak

    3. 1,2-Bis(phosphino)Ethane (pages 10–14)

      R. Craig Taylor, Douglas B. Walters, E. R. Wonchoba and G. W. Parshall

    4. Tetramethyldiphosphine and Flexible Aliphatic (dimethylphosphino) Ligands (pages 14–23)

      G. Kordosky, B. R. Cook, John Cloyd, Jr, Devon W. Meek, G. W. Parshall and E. R. Wonchoba

    5. Amido(Phosphonitrilic Chloride–Cyclic Trimer) and 1,1-Diamido(Phosphonitrilic Chloride–Cyclic Trimer) (pages 23–27)

      Gerald R. Feistel, Marlene K. Feldt, Ronald L. Dieck, Therald Moeller, Gary L. Lundquist and C. David Schmulbach

  3. Part II: Chapter Two NON-TRANSITION-METAL COMPOUNDS

    1. Perchloryl Fluoride (pages 29–33)

      C. A. Wamser, B. Sukornick, W. B. Fox, D. Gould, A. F. Clifford and J. W. Thompson

    2. Chlorodifluoroamine and Difluorodiazene (pages 34–39)

      Leon M. Zabrowski, Ronald A. De Marco, Jean'Ne M. Shreeve and Lustig Max

    3. Bis(Trifluoromethyl) Sulfoxide (pages 42–47)

      Dennis T. Sauer, Jean'ne M. Shareeve and Max Lustig

    4. Aluminum Trihydride-diethyl etherate: (Etherated Alane) (pages 47–52)

      D. L. Schmidt, C. B. Roberts, P. F. Reigler, M. F. Lemanski and E. P. Schram

    5. Trimethylammonium Tetraphenylborate: (A Ready Source of Triphenylborane) (pages 52–55)

      K. E. Reynard, R. E. Sherman, Hampton D. Smith, L. F. Hohnstedt, G. Gassenheimer and T. Wartik

    6. Tetrakis(Acetato)di-μ-amido-diborane (pages 55–56)

      D. T. Haworth, L. A. Melcher and K. Niedenzu

  4. Part II: Chapter two NON-TRANSITION-METAL COMPOUNDS

    1. Dioxygenyl Salts (pages 39–42)

      Jacob Shamir, Jehuda Binenboym, J. G. Malm and C. W. Williams

  5. Part III: Chapter Three TRANSITION-METAL COMPLEXS

    1. A General Nonaqueous Preparation of Cobalt (III) and Nickel (II) Diamine and Triamine Complexes (pages 57–63)

      Karl H. Pearson, William R. Howell, Paul E. Reinbold, Stanley Kirschner, J. W. Hart, J. Kim, R. Parker, S. Yassinzadeh and C. David Schmulbach

    2. Dianionobis(Ethylenediamine) Cobalt(III) Complexes (pages 63–77)

      J. Springbørg, C. E. Schäffer, John M. Preston and Bodie Douglas

    3. Bis(Ethylenediamine)Sulfito Complexes of Cobalt(III) (pages 77–81)

      Robert D. Hargens, Woonza Min, Robert C. Henney, T. M. Brown and A. Galliart

    4. Nitrosyliron, -Cobalt, and -Nickel Iodides (pages 81–89)

      B. Haymore, R. D. Feltham, B. E. Morris and R. A. Clement

    5. Potassium Trichloro(Ethylene)Platinate(II): (Zeise's Salt) (pages 90–92)

      P. B. Chock, J. Halpern, F. E. Paulik, Saul I. Shupack and Thomas P. Deangelis

    6. Chlorobis(Cyclooctene)Rhodium(I) and -Iridium(I) Complexes (pages 92–95)

      A. Vander Ent, A. L. Onderdelinden and Robert A. Schunn

    7. Copper(I) Ammonium Tetrathiomolybdate(VI) (pages 95–97)

      M. J. Redman and Ross H. Plovnick

  6. Part IV: Chapter Four SOME SIGNIFICANT SOLIDS: HALIDES AND OXYHALIDES

    1. Iron(II) Halides (pages 99–104)

      G. Winter, D. W. Thompson and J. R. Loehe

    2. Tungsten Oxyhalides (pages 109–122)

      J. Tillack, T. M. Brown and H. Schäfer

    3. Indium(III) Oxyfluoride: (Indium (III) Oxide Fluoride) (pages 123–126)

      B. Chamberland and J. Portier

    4. Strontium Chloride Phosphate and Vanadate(V) (pages 126–130)

      L. H. Brixner, R. Kershaw and A. Wold

  7. Part IV: Chapter Four SOME SIGNIFICANT SOLIDS: HALIDES AND OXYHALIDES

    1. Niobium(IV) Fluoride and Niobium(V) Fluoride (pages 105–109)

      Frank P. Gortsema, James B. Beal and Karl Schmidt

  8. Part IV: Chapter Four SOME SIGNIFICANT SOLIDS: OXIDES

    1. Niobium Monoxide (pages 131–134)

      T. B. Reed, E. R. Pollard, L. E. Lonney, R. E. Loehman and J. M. Honig

    2. Magnesium Chromite: (Magnesium Chromium (III) Oxide) (pages 134–139)

      W. Kunnmann and D. Bellavance

    3. Silver Ferrate(III) (pages 139–142)

      William J. Croft, Nigel C. Tombs and R. D. Shannon

    4. Barium Titanate, BaTiO3: (Barium Titanium (IV) Oxide) (pages 142–143)

      Francis S. Galasso and Michael Kestigan

    5. Bismuth Titanate, Bi4 Ti3 O12: (Bismuth Titanium Oxide) (pages 144–145)

      Francis S. Galasso and Michael Kestigian

    6. Cadmium Rhenium(V) Oxide, Cd2 Re2 O7 (pages 146–148)

      John M. Longo, Paul C. Donohue, Donald A. Batson, D. P. Kelly and A. W. Sleight

    7. Molybdenum(IV) Oxide and Tungsten(IV) Oxide Single Crystals (pages 149–152)

      Lawrence E. Conroy, Lina Ben-Dor, R. Kershaw and A. Wold

  9. Part IV: Chapter Four SOME SIGNIFICANT SOLIDS: CHALCOGENIDES

    1. Rare-Earth Sesquisulfides, Ln2 S3 (pages 152–155)

      A. W. Sleight, D. P. Kelly, R. Kershaw and A. Wold

    2. Cadmium Chromium(III) Selenide, CdCr2 Se4 (pages 155–157)

      Arthur W. Sleight and Harry L. Pinch

    3. Growth of Cobalt Disulfide Single Crystals (pages 157–160)

      R. J. Bouchard, R. Kershaw and A. Wold

    4. Chalcogenide Halides of Copper, Gold, Mercury, Antimony, and Bismuth (pages 160–173)

      A. Rabenau, H. Rau, R. Kershaw and A. Wold

  10. Part IV: Chapter Four SOME SIGNIFICANT SOLIDS: PHOSPHIDES AND SILICIDES

    1. Pyrite Type of Silicon Diphosphide (pages 173–176)

      P. C. Donohue, J. Ferretti and A. Wold

  11. Part IV: Chapter Four SOME SIGNIFICANT SOLIDS: PHOSPHIDES AND SILICIDES

    1. Single Crystals of Iron Monophosphide (pages 176–182)

      David W. Bellavance, Aaron Wold and Walter Kunnamann

    2. Copper-Solvent Flux Growth of Manganese Monosilicide (pages 182–184)

      Vancliff Johnson, Arlington Finley and Aaron Wold

  12. Part IV: Chapter Four SOME SIGNIFICANT SOLIDS: HYDRIDES

    1. Single-Crystal Cerium Hydrides (pages 184–192)

      George G. Libowitz, John G. Pack and C. E. Lundin

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      Index of Contributers (pages 195–197)

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      Subject Index (pages 199–221)

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      Formula Index (pages 223–237)

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