Inorganic Syntheses, Volume 29

Inorganic Syntheses, Volume 29

Editor(s): Russell N. Grimes

Published Online: 5 JAN 2007

Print ISBN: 9780471544708

Online ISBN: 9780470132609

DOI: 10.1002/9780470132609

About this Book

The volumes in this continuing series provide a compilation of current techniques and ideas in inorganic synthetic chemistry. Includes inorganic polymer syntheses and preparation of important inorganic solids, syntheses used in the development of pharmacologically active inorganic compounds, small-molecule coordination complexes, and related compounds. Also contains valuable information on transition organometallic compounds including species with metal-metal cluster molecules. All syntheses presented here have been tested.

Table of contents

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    2. Xenon Tetrafluoride (pages 4–6)

      Karel Lutar, Andrej Šmalc, Boris Žemva and Scott A. Kinkead

    3. Chlorine Pentafluoride (pages 7–8)

      Karel Lutar, Andrej Šmalc, Boris Žemva and Scott A. Kinkead

    4. Krypton Difluoride (pages 11–15)

      Andrej Šmalc, Karel Lutar, Boris Žemva and Scott A. Kinkead

    5. Tetrakis (2,4,6–Trimethylphenyl)Disilene (Tetramesityldisilene) (pages 19–24)

      Robin P. Tan, Gregory R. Gillette, Howard B. Yokelson, Robert West and Philip Boudjouk

    6. Hexamethyldisilathiane (pages 30–32)

      Jeung-Ho So, Philip Boudjouk, Harry H. Hong and William P. Weber

    7. Pentafluoro(Isocyanato)-λ6-Sulfane (SF5N=C=O) (pages 38–40)

      Joseph S. Thrasher, Matthew Clark, Jon B. Nielsen, Carlos Alvarado, Mark T. Anderson, Günther Steinke, Thomas Meier and Rüdiger Mews

    8. Trimethylamine-Tribromoborane (pages 51–54)

      Milap A. Mathur, Dennis A. Moore, Ronald E. Popham, Harry H. Sisler, Shawn Dolan and Sheldon G. Shore

    9. Polycyclic Borazines (pages 57–60)

      D. T. Haworth, G.-Y. Lin Kiel, Lee J. Todd and Mark W. Baize

    10. 1,5-Cyclooctanediylborylsulfides (pages 60–69)

      Roland Köster, Günter Seidel, Walter Siebert and Bernd Gangnus

    11. 1,5-Cyclooctanediylborylselenides (pages 70–77)

      Roland Köster, Günter Seidel, Mohamed Yalpani, Walter Siebert and Bernd Gangnus

    12. Trimethylamine-Diethyl-1-Propynylborane and Diethyl-1-Propynylborane (pages 77–82)

      Roland Köster, Heinz Josef Horstschäfer, Günter Seidel, Walter Siebert and Bernd Gangnus

    13. Niobium(III) and (IV) Halide Complexes (pages 119–123)

      Steven F. Pedersen, Jack B. Hartung, Eric J. Roskamp, Peter S. Dragovich, Charles J. Ruffing and Bruce A. Klein

    14. Ammonium Hexachloromolybdate(III) (pages 127–129)

      Takashi Shibahara, Mikio Yamasaki, Abdul K. Mohammed and Andrew W. Maverick

    15. Nitrido and Oxo Complexes of Rhenium(V) (pages 146–150)

      B. Patrick Sullivan, John C. Brewer, Harry B. Gray, Douglas Linebarrier and James M. Mayer

    16. Thionitrosyl Complexes of Ruthenium(II) (pages 161–164)

      K. C. Jain, U. C. Agarwala, T. W. Dekleva, P. Legzdins and J. C. Oxley

    17. trans-Dichloro Tetramine Complexes of Ruthenium(III) (pages 164–167)

      Chi-Ming Che, Tai-Chu Lau, Chung-Kwong Poon, Jill Grantham and Thomas G. Richmond

    18. Resolution of the Dodecaamminehexa-μ-Hydroxo-Tetracobalt(III) Ion (pages 169–174)

      Takaji Yasui, Tomoharu Ama, George B. Kauffman, Dušan J. Radanović and Miloš I. Djuran

    19. trans-Dicarbonyl-Di-μ-Iodo-Diiododiplatinum(II) (pages 188–189)

      Bianca Patrizia Andreini, Daniela Belli Dell'Amico, Fausto Calderazzo, Nicola Pasqualetti, Allen L. Seligson and William C. Trogler

    20. Large-Scale Synthesis of 1,2,3,4,5-Penta-Methylcyclopentadiene (pages 193–198)

      Carol M. Fendrick, Larry D. Schertz, Eric A. Mintz, Tobin J. Marks, T. E. Bitterwolf, P. A. Horine, T. L. Hubler, J. A. Sheldon and D. D. Belin

    21. η3-Allylhydridobis[Ethylenebis (Diphenylphosphine)]Molybdenum(II) (pages 201–203)

      Christopher J. Bischoff, John M. Hanckel, Maria M. Ludvig, Marcetta Y. Darensbourg, M. Maciejewski and M. Rakowski Dubois

    22. Bis(η5-Cyclopentadienyl)Molybdenum(IV) Complexes (pages 204–211)

      Ned D. Silavwe, Michael P. Castellani, David R. Tyler, Mark A. Beck, Joseph D. Lichtenhan and Nancy M. Doherty

    23. Cyclopentadienyl Rhenium Complexes (pages 211–225)

      Francine Agbossou, Edward J. O'Connor, Charles M. Garner, N. Quirós Méndez, Jesús M. Fernández, Alan T. Patton, James A. Ramsden, J. A. Gladysz, Joseph M. O'Connor, Tracy Tajima and Kevin P. Gable

    24. Mixed-Metal-Gold Phosphine Cluster Compounds (pages 279–298)

      A. M. Mueting, B. D. Alexander, P. D. Boyle, A. L. Casalnuovo, L. N. Ito, B. J. Johnson, L. H. Pignolet, M. Leeaphon, K. E. Meyer, R. A. Walton, D. M. Heinekey and T. G. P. Harper

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