A High-performance Modular Data System for Fourier Transform Ion Cyclotron Resonance Mass Spectrometry

Authors

  • Michael W. Senko,

    1. Center for Interdisciplinary Magnetic Resonance, National High Magnetic Field Laboratory, 1800 E. Paul Dirac Drive, Florida State University, Tallahassee, FL 32310 USA
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  • Jesse D. Canterbury,

    1. Center for Interdisciplinary Magnetic Resonance, National High Magnetic Field Laboratory, 1800 E. Paul Dirac Drive, Florida State University, Tallahassee, FL 32310 USA
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  • Shenheng Guan,

    1. Center for Interdisciplinary Magnetic Resonance, National High Magnetic Field Laboratory, 1800 E. Paul Dirac Drive, Florida State University, Tallahassee, FL 32310 USA
    Current affiliation:
    1. Department of Chemistry, Florida State University, Tallahassee, FL 32310 USA
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  • Alan G. Marshall

    Corresponding author
    1. Center for Interdisciplinary Magnetic Resonance, National High Magnetic Field Laboratory, 1800 E. Paul Dirac Drive, Florida State University, Tallahassee, FL 32310 USA
    Current affiliation:
    1. Department of Chemistry, Florida State University, Tallahassee, FL 32310 USA
    • Center for Interdisciplinary Magnetic Resonance, National High Magnetic Field Laboratory, 1800 E. Paul Dirac Drive, Florida State University, Tallahassee, FL 32310 USA
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Abstract

The three major components of a Fourier-transform ion cyclotron resonance (FT-ICR) mass spectrometer include the vacuum system (including ion source), the magnet and a data system capable of performing the necessary instrument control for desired experiments. Most previous FTICR systems have used commercial data systems based on custom-built electronics controlled by proprietary mini-computers developed in the early 1980's. Here we present a high-performance data system based on a personal computer running user-friendly Windows software and readily available commercial components contained in a VXI chassis and a minimal complement of simple custom electronics. The system uses a VXI pattern generator to control all aspects of the experiment. The flexibility of the pattern generator allows for performance of all current FTICR experimental sequences.

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