4. Preparative Procedures

  1. Saul Patai Professor
  1. J. W. Timberlake and
  2. J. C. Stowell

Published Online: 22 JUL 2004

DOI: 10.1002/0470023414.ch4

Hydrazo, Azo and Azoxy Groups, Volume 1 and Volume 2 (1975)

Hydrazo, Azo and Azoxy Groups, Volume 1 and Volume 2 (1975)

How to Cite

Timberlake, J. W. and Stowell, J. C. (2004) Preparative Procedures, in Hydrazo, Azo and Azoxy Groups, Volume 1 and Volume 2 (1975) (ed S. Patai), John Wiley & Sons, Ltd, Chichester, UK. doi: 10.1002/0470023414.ch4

Editor Information

  1. The Hebrew University, Jerusalem, Israel

Author Information

  1. Louisiana State University in New Orleans, New Orleans, Louisiana, U.S.A.

Publication History

  1. Published Online: 22 JUL 2004
  2. Published Print: 1 JAN 1975

Book Series:

  1. PATAI'S Chemistry of Functional Groups

Book Series Editors:

  1. Saul Patai

Series Editor Information

  1. The Hebrew University, Jerusalem, Israel

ISBN Information

Print ISBN: 9780471669241

Online ISBN: 9780470023419

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Summary

This chapter contains sections titled:

  • Preparation of Hydrazines

    • Alkylations

      • Alkylation of Hydrazine and Alkyl Hydrazines

      • Alkylation of N,N′-diacylhydrazines

      • Alkylation of Acylhydrazines

    • Lithium Reagent Addition to Azo Compounds

    • Grignard Reagent Addition to Hydrazones

    • Cycloaddition Reactions of Azo Compounds

    • Reductions

      • Reduction of N-nitroso Compounds

      • Reduction of Azines, Hydrazones, and Azo Compounds

      • Reduction of Acylhydrazines

    • N-amination

    • Hydrazines from Diaziridines

    • Hydrazines from Ureas and Sulphamides

  • Preparation of Acyclic Azoalkanes

    • Oxidation of 1,2-dialkylhydrazines

    • Oxidation of Amines

    • Oxidation of Ureas

    • from Hydrazodicarboxylates

    • Oxidation of N,N-dialkylsulphamides

  • Preparation of Azoxy Compounds

    • Oxidation of Azo Compounds

    • Reduction of Azodioxy Compounds

    • Condensation of Nitroso Compounds with Hydroxylamines

    • Alkylation of Diazotates

    • Grignard Reagent Displacements on Diimide N-oxides

    • Photochemical Syntheses

  • References