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Appendix to Volume 2: Experimental Procedures for the Functionalization of Cellulose

  1. Prof. Dr. D. Klemm1,
  2. Prof. Dr. B. Philipp2,
  3. Dr. T. Heinze1,
  4. Dr. U. Heinze1 and
  5. Dr. W. Wagenknecht2

Published Online: 1 JUN 2004

DOI: 10.1002/3527601937.app1

Comprehensive Cellulose Chemistry: Functionalization of Cellulose, Volume 2

Comprehensive Cellulose Chemistry: Functionalization of Cellulose, Volume 2

How to Cite

Klemm, D., Philipp, B., Heinze, T., Heinze, U. and Wagenknecht, W. (1998) Appendix to Volume 2: Experimental Procedures for the Functionalization of Cellulose, in Comprehensive Cellulose Chemistry: Functionalization of Cellulose, Volume 2, Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim, FRG. doi: 10.1002/3527601937.app1

Author Information

  1. 1

    Friedrich-Schiller-Universität Jena, Institut für Organische und Makromolekulare Chemie, Humboldtstraße 10, 07743 Jena, Germany

  2. 2

    Max-Planck-Institut für Kolloid- und Grenzflächenforschung, Kantstraße 55, 14513 Teltow-Seehof, Germany

Publication History

  1. Published Online: 1 JUN 2004
  2. Published Print: 14 MAY 1998

ISBN Information

Print ISBN: 9783527294893

Online ISBN: 9783527601936

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Summary

This appendix contains sections titled:

  • Preparation of FeTNa solvent for cellulose

  • Dissolution of cellulose in N,N-dimethylacetamide (DMA)/LiCl

  • Preparation of a cellulose trinitrate without significant chain degradation

  • Sulfation of cellulose with SO3–DMF

  • Cellulose sulfate, synthesis via cellulose trifluoroacetate in DMF

  • Cellulose sulfate, synthesis via trimethylsilylcellulose in THF

  • Preferentially C-6-substituted cellulose sulfate via an acetate sulfate mixed ester

  • Predominantly C-2/C-3-substituted cellulose sulfates

  • Cellulose phosphate from a partially substituted cellulose acetate

  • Preparation of a cellulose fiber xanthogenate and a cellulose xanthogenate solution

  • Cellulose tricarbanilate

  • Cellulose phenylcarbamate, synthesis via cellulose trifluoroacetate inpyridine

  • Cellulose formate, synthesis in HCOOH/POCl3

  • Laboratory procedure for the preparation of cellulose triacetate by fiber acetylation

  • Acetylation of bacterial cellulose

  • Site-selective deacetylation of cellulose triacetate

  • Cellulose dichloroacetate, synthesis with dichloroacetic acid/POCl3

  • Cellulose trifluoroacetate (DS = 1.5), synthesis with TFA/TFAA

  • Cellulose methoxyacetates, synthesis in DMA/LiCl

  • Cellulose-4-nitrobenzoate, synthesis via cellulose trifluoroacetate catalyzed with p-tosyl chloride

  • Cellulose-4-nitrobenzoate, synthesis via cellulose trifluoroacetate with 4-nitro-benzoic acid imidazolide

  • Cellulose tosylate, homogeneous synthesis in DMA/LiCl

  • 2,3-Di-O-methylcellulose

  • Carboxymethylcellulose, heterogeneous synthesis in isopropanol/water

  • Carboxymethylcellulose, synthesis in DMA/LiCl

  • Carboxymethylcellulose, synthesis via cellulose trifluoroacetate in DMSO

  • 6-O-Triphenylmethyl (trityl) cellulose, homogeneous synthesis in DMA/LiCl

  • 2,3-O-Carboxymethyl-6-O-triphenylmethylcellulose, synthesis via 6-O-tritylcellulose in DMSO

  • Detritylation of 2,3-O-carboxymethyl-6-O-triphenylmethyl cellulose

  • Crosslinking of cellulose powder with epichlorohydrin

  • Organosoluble cyanoethylcellulose

  • Trimethylsilylcellulose, synthesis in pyridine/THF

  • Trimethylsilylcellulose, synthesis in DMA/LiCl

  • Celluloses esters, synthesis via trimethylsilylcellulose, general procedure without solvents

  • 6-O-Thexyldimethylsilylcellulose

  • 2,6-Di-O-thexyldimethylsilylcellulose

  • 6-O-Thexyldimethylsilyl-2,3-di-O-methylcellulose

  • Trimethylsilylcellulose methoxyacetate: synthesis via cellulose methoxyacetate in DMA

  • 6-Carboxycellulose, homogeneous synthesis with phosphoric acid