Disodium Tris(Tetrabutylammonium) [β-Hexatricontaoxo (μ12-Tetraoxosilicato) (10,11,12-Triniobiumnonatungsten)Ato (7–)] (η5-Pentamethylcyclopentadienyl) Rhodate (5–), Na2(Bu4N)3[Rh[β-Nb3 SiW9O40]{η5-C5(CH3)5}]

  1. Russell N. Grimes
  1. R. G. Finke1,
  2. K. Nomiya1,
  3. C. A. Green1,
  4. M. W. Droege1 and
  5. A. R. Siedle2

Published Online: 5 JAN 2007

DOI: 10.1002/9780470132609.ch55

Inorganic Syntheses, Volume 29

Inorganic Syntheses, Volume 29

How to Cite

Finke, R. G., Nomiya, K., Green, C. A., Droege, M. W. and Siedle, A. R. (1992) Disodium Tris(Tetrabutylammonium) [β-Hexatricontaoxo (μ12-Tetraoxosilicato) (10,11,12-Triniobiumnonatungsten)Ato (7–)] (η5-Pentamethylcyclopentadienyl) Rhodate (5–), Na2(Bu4N)3[Rh[β-Nb3 SiW9O40]{η5-C5(CH3)5}], in Inorganic Syntheses, Volume 29 (ed R. N. Grimes), John Wiley & Sons, Inc., Hoboken, NJ, USA. doi: 10.1002/9780470132609.ch55

Author Information

  1. 1

    Department of Chemistry, University of Oregon, Eugene, OR 97403.

  2. 2

    3M Central Research Laboratories, St. Paul, MN 55144.

Publication History

  1. Published Online: 5 JAN 2007
  2. Published Print: 1 JAN 1992

Book Series:

  1. Inorganic Syntheses

ISBN Information

Print ISBN: 9780471544708

Online ISBN: 9780470132609

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Keywords:

  • tetrabutylammonium hydroxide;
  • hydrous niobium oxide;
  • ethyl acetate;
  • hydrogen ion;
  • decomposition

Summary

This chapter contains sections titled:

  • [Bu4N]6H2[(μ4-O)3[β-Nb3SiW9O37]2]

  • Na2(Bu4N)3[Rh[β-Nb3SiW9O40](η5-C5Me5)]