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Unsymmetric tetrathifulvalene (TTF) derivatives, especially when fused with 1,3-dithiol-2-ylidenes (DT-TTFs), have yielded a large number of metallic salts and even some superconductors. The synthesis and characterization of teh methyl-substituted DT-TTF MeDTDM (see Figure) are reported as part of the search for new superconductors, the conductivities and X-ray structure analysis of the new metallic salts being emphasized.