High-Pressure, High-Temperature Formation of Phase-Pure Monoclinic Zirconia Nanocrystals Studied by Time-Resolved in situ Synchrotron X-Ray Diffraction

Authors

  • Martin Bremholm,

    1. Center for Energy Materials Department of Chemistry and iNANO Aarhus University Langelandsgade140, 8000 Aarhus C (Denmark)
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  • Jacob Becker-Christensen,

    1. Center for Energy Materials Department of Chemistry and iNANO Aarhus University Langelandsgade140, 8000 Aarhus C (Denmark)
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  • Bo Brummerstedt Iversen

    Corresponding author
    1. Center for Energy Materials Department of Chemistry and iNANO Aarhus University Langelandsgade140, 8000 Aarhus C (Denmark)
    • Center for Energy Materials Department of Chemistry and iNANO Aarhus University Langelandsgade140, 8000 Aarhus C (Denmark).
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Abstract

original image

High-pressure, high-temperature, time- resolved X-ray diffraction is used to study the gel formation of aqueous zirconium acetate, and the crystallization into phase-pure, monoclinic, anisotropic nanocrystals.

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