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In this Special Issue of Advanced Materials, Guest Editor Professor Jennifer A. Lewis presents an overview of the cutting-edge research being carried out at Frederick Seitz Materials Research Laboratory at the University of Illinois at Urbana Champaign (UIUC). The issue is divided into three broad themes: materials synthesis and assembly; functional materials for energy harvesting, transport, and storage; and advanced techniques for materials characterization, and provides a fascinating glimpse inside one of the world's leading centers of materials science research.