This work was supported by Grants-in-Aid for Scientific Research, Young Scientists, and COE Research from the Ministry of Education, Culture, Sports, Science, and Technology, Japan. We thank Prof. Masaki Shimizu (Department of Material Chemistry, Kyoto University) and Dr. Yasuyuki Ura (Department of Energy and Hydrocarbon Chemistry, Kyoto University) for generous help with the X-ray crystallographic analysis and for teaching us how to purify air-sensitive compounds, respectively. We also acknowledge Mr. Hiroshi Hata and Prof. Naoki Aratani and Prof. Hiroshi Shinokubo (Department of Science, Kyoto University) for measuring UV/Vis and fluorescence spectra. Chlorodicyclohexylphosphane was a gift from Hokko Chemical Industry Co., Ltd.
Synthesis of (E)-1,2-Diphosphanylethene Derivatives from Alkynes by Radical Addition of Tetraorganodiphosphane Generated In Situ†
Article first published online: 2 FEB 2005
Copyright © 2005 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim
Volume 117, Issue 11, pages 1722–1724, March 4, 2005
How to Cite
Sato, A., Yorimitsu, H. and Oshima, K. (2005), Synthesis of (E)-1,2-Diphosphanylethene Derivatives from Alkynes by Radical Addition of Tetraorganodiphosphane Generated In Situ. Angew. Chem., 117: 1722–1724. doi: 10.1002/ange.200462603
- Issue published online: 2 MAR 2005
- Article first published online: 2 FEB 2005
- Manuscript Received: 14 NOV 2004
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