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Continuous In Situ Generation, Separation, and Reaction of Diazomethane in a Dual-Channel Microreactor

Authors

  • Dr. Ram Awatar Maurya,

    1. National Creative Research Center of Applied Microfluidic, Chemistry, Chungnam National University, Daejeon, 305-764 (South Korea)
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    • Both authors contributed equally to this work.

  • Dr. Chan Pil Park,

    1. National Creative Research Center of Applied Microfluidic, Chemistry, Chungnam National University, Daejeon, 305-764 (South Korea)
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    • Both authors contributed equally to this work.

  • Jang Han Lee,

    1. National Creative Research Center of Applied Microfluidic, Chemistry, Chungnam National University, Daejeon, 305-764 (South Korea)
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  • Prof. Dr. Dong-Pyo Kim

    Corresponding author
    1. National Creative Research Center of Applied Microfluidic, Chemistry, Graduate School of Analytical Science and Technology, Chungnam National University, Daejeon, 305-764 (South Korea), Fax: (+82) 42-823-6665 http://www.camc.re.kr
    • National Creative Research Center of Applied Microfluidic, Chemistry, Graduate School of Analytical Science and Technology, Chungnam National University, Daejeon, 305-764 (South Korea), Fax: (+82) 42-823-6665 http://www.camc.re.kr
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  • This work was supported by a National Research Foundation of Korea (NRF) grant funded by the Korean government(MEST) (No. 2008-0061983).

Abstract

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Ein bissiger Hund: Die bedarfsgesteuerte kontinuierliche In-situ-Erzeugung, Trennung und Reaktion von Diazomethan in einem Zweikanalmikroreaktor (siehe Bild; Diazald=N-Methyl-N-nitroso-p-toluolsulfonamid) ermöglicht die Durchführung zahlreicher Diazomethanreaktionen unter Vermeidung der gängigsten Probleme bei Herstellung, Handhabung, Transport und Zersetzung.

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