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Preparation of Thiocarbonyl Compounds Containing Isotopic Sulfur Labels

Authors

  • Dipl.-Chem. Claus-Peter Klages,

    1. Institut für Organische Chemie und Biochemie der Universität, Martin-Luther-King-Platz 6, D-2000 Hamburg 13 (Germany)
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  • Prof. Dr. Jürgen Voss

    Corresponding author
    1. Institut für Organische Chemie und Biochemie der Universität, Martin-Luther-King-Platz 6, D-2000 Hamburg 13 (Germany)
    • Institut für Organische Chemie und Biochemie der Universität, Martin-Luther-King-Platz 6, D-2000 Hamburg 13 (Germany)
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  • This work was supported by the Fonds der Chemischen Industrie.

Abstract

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Sulfur-sulfur exchange in thiocarbonyl compounds, which permits isotopic substitutions, can be accomplished by heating of R1R2C[DOUBLE BOND]S with isotopically enriched sulfur. Se can likewise be replaced by *S.

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