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Keywords:

  • asymmetric synthesis;
  • Heck;
  • reactions;
  • NMR spectroscopy;
  • palladium
Thumbnail image of graphical abstract

Double isomerization results in a Pd-alkyl compound with unexpected structure, which is stable until −40°, from the reaction of the Pd complex shown on the right with 2,3-dihydrofuran. The course of the asymmetric Heck reaction was followed by NMR spectroscopy.

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