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    Crystal Data for 1: C15H21ClNO4, Mr=313.11, monoclinic space group, P21, a=10.4805(6), b=24.2085(13), c=12.5163(7) Å, β=108.603(10)°, V=3009.7(3) Å3, Z=8, ρcalcd=1.385 g cm−3; Mo radiation, λ=0.71073 Å, μ=0.269 mm−1, T=−100 K. 25 627 data (13 056 unique, Rint=0.0146, θ<27.52°) were collected on a Bruker SMART APEX CCD X-ray diffractometer. The structure was solved by direct methods and refined by full-matrix least-squares on F2 values of all data (G. M. Sheldrick, SHELXTL Manual) to give wR2=0.0824, conventional R=0.0313 for F values of 12 747 reflections, S=1.037 and 773 parameters. Residual electron density max/min 0.448/−0.232 e Å−3. CCDC-183413 (1) contains the supplementary crystallographic data for this paper. These data can be obtained free of charge via www.ccdc.cam.ac.uk/conts/retrieving.html (or from the Cambridge Crystallographic Data Centre, 12 Union Road, Cambridge CB2 1EZ, UK; fax: (+44) 1223-336-033; or deposit@ccdc.cam.ac.uk).
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    We gratefully acknowledge K. Lloyd, S. Glaser, B. Miller, Nereus Pharmaceuticals Inc., for providing proteasome inhibition data.