Scientific advice by Jacco van Beek, René Verel, and Urban Meier and financial support by the Schweizerischer Nationalfonds, the ETH Zurich, and the Kommission für Technologie und Innovation is acknowledged.
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Communication
One- and Two-Dimensional NMR Spectroscopy with a Magnetic-Resonance Force Microscope†
Article first published online: 16 OCT 2008
DOI: 10.1002/anie.200802978
Copyright © 2008 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim
Additional Information
How to Cite
Eberhardt, Kai W., Degen, Christian L., Hunkeler, A. and Meier, Beat H. (2008), One- and Two-Dimensional NMR Spectroscopy with a Magnetic-Resonance Force Microscope. Angew. Chem. Int. Ed., 47: 8961–8963. doi: 10.1002/anie.200802978
- †
Publication History
- Issue published online: 28 OCT 2008
- Article first published online: 16 OCT 2008
- Manuscript Received: 21 JUN 2008
Funded by
- Schweizerischer Nationalfonds
- ETH Zurich
- Kommission für Technologie und Innovation
Keywords:
- imaging;
- microimaging;
- microscopy;
- NMR spectroscopy
At the micrometer scale: Chemical interactions at the atomic level have been characterized with localized spectroscopy by using magnetic-resonance force microscopy to locate slices of 2.0 μm thickness in a heterogeneous sample (see picture). To recover the chemical-shift information, the field gradient was temporarily switched off by removing its source mechanically. This technique allows high-resolution one- and two-dimensional NMR spectra to be recorded.