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Detection of Structural Elements of Different Zeolites in Nucleating Solutions by Electrospray Ionization Mass Spectrometry

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  • The authors acknowledge partial financial support by the Leibniz program of the Deutsche Forschungsgemeinschaft (DFG), in addition to the basic funding provided by the Max-Planck-Gesellschaft (MPG). We thank Dr. C. Weidenthaler and Dr. C. W. Lehmann for their support in the X-ray analyses as well as Ms. S. Palm for her support in the EDX analyses.

Abstract

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Building blocks in solution: Characteristic structural elements of the germanium-containing zeolites ZSM-5, polymorph C of zeolite Beta, and zeolite A (see picture) are identified in solution immediately before nucleation. The conditions of the reaction direct the polycondensation of silicate towards specific structures at the solution stage.

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