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Keywords:

  • alkenes;
  • copper;
  • homogeneous catalysis;
  • iron;
  • synthetic methods
Thumbnail image of graphical abstract

Direct access: The title reaction has been developed under mild reaction conditions (see scheme; DMSO=dimethyl sulfoxide). This reaction can be effectively scaled up and offers not only a green and attractive approach to β-ketophosphonates, but also a useful example of direct incorporation of an oxygen atom from dioxygen into organic frameworks.