Both authors contributed equally to this work.
Continuous In Situ Generation, Separation, and Reaction of Diazomethane in a Dual-Channel Microreactor†
Article first published online: 25 MAY 2011
Copyright © 2011 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim
Angewandte Chemie International Edition
Volume 50, Issue 26, pages 5952–5955, June 20, 2011
How to Cite
Maurya, R. A., Park, C. P., Lee, J. H. and Kim, D.-P. (2011), Continuous In Situ Generation, Separation, and Reaction of Diazomethane in a Dual-Channel Microreactor. Angew. Chem. Int. Ed., 50: 5952–5955. doi: 10.1002/anie.201101977
This work was supported by a National Research Foundation of Korea (NRF) grant funded by the Korean government(MEST) (No. 2008-0061983).
- Issue published online: 15 JUN 2011
- Article first published online: 25 MAY 2011
- Manuscript Received: 21 MAR 2011
- National Research Foundation of Korea
- Korean government(MEST). Grant Number: 2008-0061983
- cascade reactions;
A fierce dog: A method for the continuous in-situ on-demand generation, separation, and reaction of diazomethane in a dual-channel microreactor has been developed (see picture; Diazald=N-methyl-N-nitroso-p-toluenesulfonamide). The microchemical system allows a variety of diazomethane reactions to be performed without the most common problems of preparation, handling, transfer, and decomposition.