Communication

Simple Proton Spectra from Complex Spin Systems: Pure Shift NMR Spectroscopy Using BIRD†

  1. Dr. Juan A. Aguilar,
  2. Dr. Mathias Nilsson,
  3. Prof. Gareth A. Morris*

Article first published online: 31 AUG 2011

DOI: 10.1002/anie.201103789

Issue

Angewandte Chemie International Edition

Angewandte Chemie International Edition

Volume 50, Issue 41, pages 9716–9717, October 4, 2011

Additional Information

How to Cite

Aguilar, J. A., Nilsson, M. and Morris, G. A. (2011), Simple Proton Spectra from Complex Spin Systems: Pure Shift NMR Spectroscopy Using BIRD. Angew. Chem. Int. Ed., 50: 9716–9717. doi: 10.1002/anie.201103789

Author Information

  1. School of Chemistry, University of Manchester, Oxford Road, Manchester, M13 9PL (UK) http://nmr.chemistry.manchester.ac.uk

*School of Chemistry, University of Manchester, Oxford Road, Manchester, M13 9PL (UK) http://nmr.chemistry.manchester.ac.uk

  1. †

    This work was supported by the Engineering and Physical Sciences Research Council (Grant Number EP/H024336/1, EP/I007989/1, and EP/E05899X/1).

Publication History

  1. Issue published online: 27 SEP 2011
  2. Article first published online: 31 AUG 2011
  3. Manuscript Received: 3 JUN 2011

Funded by

  • Engineering and Physical Sciences Research Council. Grant Numbers: EP/H024336/1, EP/I007989/1, EP/E05899X/1

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Keywords:

  • bilinear rotation decoupling;
  • homonuclear decoupling;
  • NMR spectroscopy;
  • pure shift NMR;
  • structure elucidation
Thumbnail image of graphical abstract

Turning multiplets into singlets: Bilinear rotation decoupling (BIRD) allows broadband homonuclear decoupling of proton NMR spectra even when spins are very strongly coupled, as in the two aromatics shown.

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