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Keywords:

  • arylamines;
  • cyclophanes;
  • electrochemistry;
  • EPR spectroscopy;
  • radical ions
Thumbnail image of graphical abstract

Double- and triple-decker oligoarylamines have been prepared and characterized by X-ray crystallography for the first time (see picture; C black, N blue). The N-dianisylaminophenyl-substituted double decker exhibited the multiredox activity, and the oxidized species were confirmed to be in high-spin states on the basis of pulsed ESR spectroscopy.