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Keywords:

  • dynamic nuclear polarization;
  • nanostructures;
  • NMR spectroscopy;
  • peptides;
  • self-assembly
Thumbnail image of graphical abstract

Supra-sensitivity: Dynamic nuclear polarization (DNP) enhanced solid-state NMR spectroscopy was performed on self-assembled peptide nanotubes. This approach yields significant experimental time savings (about five orders of magnitude; see picture) and was used to exemplify the feasibility of supramolecular structural studies of organic nanoassemblies at an atomic scale using DNP-enhanced solid-state NMR spectroscopy.