Rapid, sensitive and specific determination of oxytetracycline residues in bovine milk and meat by CAD MIKES analysis at the 1 ppb level
Article first published online: 11 APR 2005
Copyright © 1985 John Wiley & Sons, Ltd.
Biological Mass Spectrometry
Volume 12, Issue 9, pages 493–496, September 1985
How to Cite
Traldi, P., Daolio, S., Pelli, B., Facino, R. M. and Carini, M. (1985), Rapid, sensitive and specific determination of oxytetracycline residues in bovine milk and meat by CAD MIKES analysis at the 1 ppb level. Biol. Mass Spectrom., 12: 493–496. doi: 10.1002/bms.1200120908
- Issue published online: 11 APR 2005
- Article first published online: 11 APR 2005
- Manuscript Accepted: 24 JUL 1984
- Manuscript Received: 18 MAY 1984
A rapid and sensitive method for the selective detection and quantification of oxytetracycline residues at the ppb level in crude extracts of bovine milk and meat is described. The technique employed is a tandem mass spectrometric method: CAD MIKE spectrometry (collisionally activated decomposition mass-analysed ion kinetic energy spectrometry). Quantification is performed by single ion monitoring of CAD species of oxytetracycline and of its internal standard.