Highly Controlled Gas/Liquid Processes in a Continuous Lab-Scale Device (pages 1042–1046)
J. J. F. van Gool, S. A. M. W. van den Broek, R. M. Ripken, P. J. Nieuwland, K. Koch and F. P. J. T. Rutjes
Version of Record online: 13 MAY 2013 | DOI: 10.1002/ceat.201200553
Gas-permeable membrane-based reactors offer safe handling of gases in a continuous-flow system. A prototype of a gas/liquid system was constructed to introduce gas in a microreactor. An integrated gas flow controller and inline FTIR analysis were used to safely handle the gas. Carboxylation of a Grignard reagent with CO2 served as a nonhazardous model reaction.