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Keywords:

  • polyhedral oligomeric silsesquioxanes;
  • zirconium;
  • hafnium;
  • polymers

Abstract

The synthesis and characterization of Zr-POSS and Hf-POSS coordination polymers were reported. The IR data and the solid-state 29Si MAS NMR indicated the existence of Si[BOND]O[BOND]M linkage. The polarized optical microscopy images and the XRD data suggested their crystalline nature.