13C–13C Chemical Shift Correlation in Rotating Solids without 1H Decoupling During Mixing

Authors

  • Christian Herbst,

    1. Molecular Biophysics/NMR spectroscopy Leibniz Institute for Age Research, Fritz Lipmann Institute, Beutenbergstrasse 11, 07745 Jena, Germany, Fax: (+49) 3641-656225
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  • Kerstin Riedel,

    1. Molecular Biophysics/NMR spectroscopy Leibniz Institute for Age Research, Fritz Lipmann Institute, Beutenbergstrasse 11, 07745 Jena, Germany, Fax: (+49) 3641-656225
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  • Jörg Leppert Dr.,

    1. Molecular Biophysics/NMR spectroscopy Leibniz Institute for Age Research, Fritz Lipmann Institute, Beutenbergstrasse 11, 07745 Jena, Germany, Fax: (+49) 3641-656225
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  • Oliver Ohlenschläger Dr.,

    1. Molecular Biophysics/NMR spectroscopy Leibniz Institute for Age Research, Fritz Lipmann Institute, Beutenbergstrasse 11, 07745 Jena, Germany, Fax: (+49) 3641-656225
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  • Matthias Görlach Dr.,

    1. Molecular Biophysics/NMR spectroscopy Leibniz Institute for Age Research, Fritz Lipmann Institute, Beutenbergstrasse 11, 07745 Jena, Germany, Fax: (+49) 3641-656225
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  • Ramadurai Ramachandran Dr.

    1. Molecular Biophysics/NMR spectroscopy Leibniz Institute for Age Research, Fritz Lipmann Institute, Beutenbergstrasse 11, 07745 Jena, Germany, Fax: (+49) 3641-656225
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  • An Assessment of Amplitude and Phase-Modulated Adiabatic RF Pulse Schemes

Abstract

original image

Adiabatic RF pulse schemes using inversion pulses with low power factor are difficult to implement but are shown to be feasible and advantageous for generating 13C–13C MAS solid-state NMR chemical shift correlation spectra via longitudinal magnetisation exchange without 1H decoupling during mixing (see figure).

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