This paper is included in the virtual special issue Monoliths available at the Journal of Separation Science website.
Organic–inorganic hybrid fluorous monolithic capillary column for selective solid-phase microextraction of perfluorinated persistent organic pollutants†
Version of Record online: 4 FEB 2013
© 2012 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim
Journal of Separation Science
Volume 36, Issue 5, pages 923–931, March 2013
How to Cite
Xiong, X., Yang, Z., Huang, Y., Jiang, L., Chen, Y., Shen, Y. and Chen, B. (2013), Organic–inorganic hybrid fluorous monolithic capillary column for selective solid-phase microextraction of perfluorinated persistent organic pollutants. J. Sep. Science, 36: 923–931. doi: 10.1002/jssc.201200913
- Issue online: 8 MAR 2013
- Version of Record online: 4 FEB 2013
- Accepted manuscript online: 27 NOV 2012 07:15PM EST
- Manuscript Accepted: 15 NOV 2012
- Manuscript Revised: 23 OCT 2012
- Manuscript Received: 29 SEP 2012
- National “863” Research Foundation. Grant Number: 2010AA023001
- National Natural Science Foundation of China. Grant Numbers: 20927005, 21005027, 21275049, 81274178
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Figure S1. Linear pressure dependence of the optimized fluorous monolithic capillary column on the flow rate of water and ACN. The pressures were normalized to a column length of 10 cm.
Figure S2-1. Adsorption isotherm of PFOS to the optimal monolith.
Figure S2-2. Adsorption isotherm of PFOA to the optimal monolith. ♦ represents PFOA was independently adsorbed to the monolith; ▲ represents adsorption isotherm of PFOA wthen PFOA and PFOS were simultaneously adsorbed to the monolith.
Table S1. Effects of composition of feed mixtures on properties of the obtained monolithic columns
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