Determination of spinosad at trace levels in bee pollen and beeswax with solid–liquid extraction and LC–ESI-MS
Version of Record online: 12 DEC 2013
© 2013 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim
Journal of Separation Science
Volume 37, Issue 3, pages 204–210, February 2014
How to Cite
Yáñez, K. P., Martín, M. T., Bernal, J. L., Nozal, M. J. and Bernal, J. (2014), Determination of spinosad at trace levels in bee pollen and beeswax with solid–liquid extraction and LC–ESI-MS. J. Sep. Science, 37: 204–210. doi: 10.1002/jssc.201301069
- Issue online: 3 FEB 2014
- Version of Record online: 12 DEC 2013
- Accepted manuscript online: 14 NOV 2013 07:59PM EST
- Manuscript Revised: 5 NOV 2013
- Manuscript Accepted: 5 NOV 2013
- Manuscript Received: 28 SEP 2013
- Spanish MARM-FEAGA (Programa Nacional Apícola 2011–2013)
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Table S1. Recoveries obtained after testing different extraction times, extractant volumes and centrifugation times of 2 g pollen and beeswax at a spiking level of 100 μg/kg.
Table S2. Repeatability and intermediate precision results. Data obtained as described in Section 'Method validation' (n = 6).
Table S3. Summarized results of advances in analytical methods for the estimation of spinosad and its ingredients in bee related matrices.
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