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Figure S1. Evolution of GPC traces of the prepared PS-TTC.

Figure S2. Evolution of GPC traces of the prepared PS-DTSC.

Figure S3. Evolution of GPC traces of the prepared PS-TDSC.

Figure S4. Evolution of GPC traces of the prepared PS-TSC.

Figure S5.1H NMR full spectra of PS-TTC obtained from TTC (Mn,GPC = 9700, Mw/Mn = 1.26) in CDCl3.

Figure S6.1H NMR full spectra of PS-DTSC obtained from DTSC (Mn,GPC = 10500, Mw/Mn = 1.17) in CDCl3.

Figure S7.1H NMR full spectra of PS-TDSC obtained from TDSC (Mn,GPC = 5800, Mw/Mn = 1.24) in CDCl3.

Figure S8.1H NMR spectra of PS-DTSC after oxidative homolysis. (Mn,GPC= 5900 g/mol, Mw/Mn= 1.17) with CDCl3 as the solvent.

Figure S9.1H NMR spectra of PS-TDSC after oxidative homolysis. (Mn,GPC= 8100 g/mol, Mw/Mn= 1.26) with CDCl3 as the solvent.

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