Intramolecular atom transfer radical coupling of macromolecular brushes
Version of Record online: 30 MAY 2013
© 2013 Wiley Periodicals, Inc.
Journal of Polymer Science Part A: Polymer Chemistry
Volume 51, Issue 17, pages 3567–3571, 1 September 2013
How to Cite
Liu, J., Lian, X., Zhao, F. and Zhao, H. (2013), Intramolecular atom transfer radical coupling of macromolecular brushes. J. Polym. Sci. A Polym. Chem., 51: 3567–3571. doi: 10.1002/pola.26760
- Issue online: 19 JUL 2013
- Version of Record online: 30 MAY 2013
- Manuscript Revised: 6 MAY 2013
- Manuscript Accepted: 6 MAY 2013
- Manuscript Received: 28 NOV 2012
- National Natural Science Foundation of China (NSFC) . Grant Numbers: 21074058 , 20874050
Additional Supporting Information may be found in the online version of this article.
Figure S1. 1H NMR spectrum of CH3-O-PEG-Br macroinitiator.
Figure S2. 1H NMR spectrum of PEG-b-PHEMA. In the 1H NMR measurement d6-DMSO was used as the solvent.
Figure S3. 1H NMR spectrum of PEG-block-poly(2-(2-bromoisobutyrnyloxy)ethyl methacrylate (PEG-b-PBIEM) macroinitiator.
Figure S4. 1H NMR spectrum of PEG-b-PBIEM350-g-PS186 macromolecular Brushes.
Figure S5. GPC traces of PEG-Br, PEG-b-PBIEM350 and PEG-b-PBIEM350-g-PS186.
Figure S6. AFM images of PEG-b-PBIEM350-g-PS186 macromolecular brushes before (a) and after (b) ATRC coupling reaction.
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