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ps3841-sup-0001-FigureS1.docWord document625KFigure S1 HPLC-HESI-MS/MS chromatograms (a Chiralcel OD-3R column, 3 µm particle size, 4.6 × 150 mm i.d.) of enantiomers of fipronil and metabolites.
ps3841-sup-0002-FigureS2.docWord document649KFigure S2 HPLC chromatogram of enantiopure S-fipronil (UV 280 nm, mobile phase: water:acetonitrile, 50:50 (V/V); column temperature, 25 °C).
ps3841-sup-0003-FigureS3.docWord document33KFigure S3 HPLC chromatogram of enantiopure R-fipronil (UV 280 nm, mobile phase: water:acetonitrile, 50:50 (V/V); column temperature, 25 °C).

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