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Zinc oxysulphate [Zn3O(SO4)2] crystallizes with a monoclinic unit cell, a = 7.867 (7), b = 6.700 (7), c = 7.374 (7) Å, β = 117.3 (1)°, Z = 2, space group P21 or P21/m, Dm = 3.89, Dx = 3.887 g cm−3. An indexed powder pattern is given.