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Fig. S1. Chemical structures of the five main HCH isomers, HeCH and their metabolites. Note that only one possible enantiomer of chiral compounds is shown for simplicity. HCH – 1,2,3,4,5,6-hexachlorocyclohexane; HeCH – 1,1,2,3,4,5,6-heptachlorocyclohexane; B1, D1, E1 – 2,3,4,5,6-pentachlorocyclohexanol; He1 – 2,3,4,4,5,6-hexachlorocyclohexanol; B2, D2, E2 – 2,3,5,6-tetrachlorocyclohexane-1,4-diol, PCCH – 2,3,4,5,6-pentachlorocyclohexene; HCCH – 1,2,3,4,5,6-hexachlorocyclohexene; A3, D3, G3 – 3,4,5,6-tetrachloro-2-cyclohexenol; G3b – 2,4,5,6-tetrachloro-2-cyclohexeneol; A4, T4, D4, G4 – 3,5,6-trichloro-2-cyclohexene-1,4-diol; He4 – 2,3,5,6-tetrachloro-2-cyclohexene-1,4-diol.

Fig. S2. EI mass spectra of the metabolites E4, D4b and He4.

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