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Behavior of Low Molecular Weight Organic Acids During Freeze Drying

Authors

  • L. GERO,

    1. Authors Gero and Smyrl are affiliated with the School of Food Science, Macdonald Campus of McGill Univ., Ste Anne de Belleuve, Québec, Canada H9X 1CO.
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  • T. G. SMYRL

    1. Authors Gero and Smyrl are affiliated with the School of Food Science, Macdonald Campus of McGill Univ., Ste Anne de Belleuve, Québec, Canada H9X 1CO.
    Search for more papers by this author

  • The authors are grateful to Agriculture Canada for financial support of this work.

ABSTRACT

The retentions of several low molecular weight organic acids (formic, acetic, propionic, lactic, n-butyric and isobutyric) were measured during the freeze drying of model solutions in which dextran was employed as the dissolved solid. Acid retentions were found to increase with initial dextran content and with a decreasing rate of sample freezing. An increase in initial acid concentration was found to decrease the percent acid retained. Sample layer thickness and the presence of additional volatiles (ethanol and hexanol) were found to have very little influence on the degree of acid retentions.

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