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Controlled Evolution of Morphology and Microstructure in Laser Interference-Structured Zirconia
Article first published online: 14 MAY 2008
DOI: 10.1111/j.1551-2916.2008.02449.x
© 2008 The American Ceramic Society
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How to Cite
Daniel, C., Armstrong, B. L., Howe, J. Y. and Dahotre, N. B. (2008), Controlled Evolution of Morphology and Microstructure in Laser Interference-Structured Zirconia. Journal of the American Ceramic Society, 91: 2138–2142. doi: 10.1111/j.1551-2916.2008.02449.x
Publication History
- Issue published online: 8 JUL 2008
- Article first published online: 14 MAY 2008
- Manuscript No. 23605. Received August 14, 2007; approved March 10, 2008.
- Abstract
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Tape-cast pseudo-cubic zirconia pellets were surface irradiated by two coherent interfering high-power short-pulse Nd:YAG laser beams. The interfering beams of the third harmonic with a wavelength of 355 nm of a 2.5-ns Q-switched laser produced a line-like intensity distribution with a periodic distance of 3.3 μm due to the selected angle between the beams. The resulting nonuniform surface heating produced a microstructure consisting of ultrafine-grained zirconia with a grain size of about 10 nm within the top 100–200 nm depth of the treated surface region due to the high cooling rates during short-pulse laser processing (up to 1010 K/s). The surface morphology closely followed the microperiodic heat treatment provided by the interfering laser beams. The pore size distribution within the periodic surface morphology ranged from a few nanometers to a maximum of half of the periodic line distances.

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