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Keywords:

  • acrylic resin;
  • glass transition temperature;
  • differential scanning calorimetry;
  • post-polymerisation treatment

doi:10.1111/j.1741-2358.2009.00312.x Glass transition temperature of hard chairside reline materials after post-polymerisation treatments

Objective:  This study evaluated the effect of post-polymerisation treatments on the glass transition temperature (Tg) of five hard chairside reline materials (Duraliner II-D, Kooliner-K, New Truliner-N, Ufi Gel hard-U and Tokuso Rebase Fast-T).

Materials and methods:  Specimens (10 × 10 × 1 mm) were made following the manufacturers’ instructions and divided into three groups (n = 5). Control group specimens were left untreated. Specimens from the microwave group were irradiated with pre-determined power/time combinations, and specimens from the water-bath group were immersed in hot water at 55°C for 10 min. Glass transition (°C) was performed by differential scanning calorimetry. Data were analysed using anova, followed by post hoc Tukey’s test (α = 0.05).

Results:  Both post-polymerisation treatments promoted a significant (< 0.05) increase in the Tg of reline material K. Materials K, D and N showed the lowest Tg (< 0.05). No significant difference between T and U specimens was observed.

Conclusion:  Post-polymerisation treatments improved the glass transition of material Kooliner, with the effect being more pronounced for microwave irradiation.