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Figure S1. 1H NMR spectrum of 1,2:3,4-di-O-isopropylidene-α-D-glucopyranose {1} measured in CDCl3.

Figure S2. 1H NMR spectrum of 4-(1,2:3,4-di-O-isopropylidene-α-D-glucopyranose)-phthalonitriles {3} measured in CDCl3.

Figure S3. (A) 1H NMR spectrum of tetra-β-glycosylated ZnPc {4} measured in DMSO-d6. (B) MALDI TOF MS of tetra-β-glycosylated ZnPc {4} in MeOH. (C, D) Expanded MALDI TOF MS of tetra-β-glycosylated ZnPc {4} in MeOH showing the isotopic distribution of the mono (C) and dimeric (D) species.

Figure S4. 1H NMR spectrum of tetra-β-glycosylated ZnPc {5} measured in DMSO-d6.

Figure S5. MALDI TOF MS spectrum of tetra-β-glycosylated ZnPc {5} in MeOH.

Figure S6. The expanded MALDI TOF MS of tetra-β-glycosylated ZnPc {5} in MeOH showing the isotopic distribution of the mono (A) and dimeric (B) species.

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