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Table S1. GC/MS Identification of the target compounds based on retention time of the quantification ion and the corresponding ratio (% in parentheses) of the qualifying ions relative to the quantification ion for each compound. Retention times, quantification and qualifying ions based on the trimethylsilate (TMS) derivatives of the target compounds.

Table S2. The concentration of the individual soluble phenolic constituents in the extracts from the three methodologies for the wild oat caryopses. Values within a row followed by the same letters are not significantly different at the P < 0·05 confidence interval.

Table S3. The concentration of the individual soluble phenolic constituents in the extracts from the three methodologies for the wild oat hulls. Values within a row followed by the same letters are not significantly different at the P < 0·05 confidence interval.

Table S4. The concentration of the individual soluble phenolic constituents in the extracts from the three methodologies for common lambsquarters seeds. Values within a row followed by the same letters are not significantly different at the P < 0·05 confidence interval.

Table S5. The concentration of the individual soluble phenolic constituents in the extracts from the three methodologies for broadleaf plantain seeds. Values within a row followed by the same letters are not significantly different at the P < 0·05 confidence interval.

Table S6. The concentration of the individual bound phenolic constituents in the extracts from the three methodologies for the seeds of three weed species. Bound phenolics were extracted by the method of Gallagher et al. (2010).

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