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jace12013-sup-0001-FigS1.tifimage/tif4724KFig. S1. X-ray diffraction data of YBiTi2O7 annealed at 873 K for 4 h (a) and Y1.5Bi0.5Ti2O7 annealed at 1023 K for 4 h (b) and 1173 K for 4 h (c).
jace12013-sup-0002-FigS2.tifimage/tif2670KFig. S2. Detail of the X-ray diffraction data in the angular range of 24.5 to 31.5° 2θ for analysis of the titania by-phases rutile and anatase of (Y1.5Bi0.5)1−xTi2O7−3x and (YBi)1−xTi2O7−3x samples annealed at 1023 or 1173 K as a function of the Ti/(Y+Bi) ratio.
jace12013-sup-0003-FigS3.tifimage/tif4833KFig. S3. STEM micrograph in dark field mode (a) and the platinum EDXS mapping (b) of (YBi)1−xTi2O7−3x 1.30 Ti/(Y+Bi) annealed at 873 K for 4 h and loaded with 3.0 wt% of platinum.
jace12013-sup-0004-FigS4.tifimage/tif2682KFig. S4. Photocatalytic activity regarding hydrogen production over (Y1.5Bi0.5)1−xTi2O7−3x calcined at 1173 K for 4 h with 0.75 wt% platinum as co-catalysts in the presence of 10 vol% methanol as sacrificial reagent.
jace12013-sup-0005-FigS5.tifimage/tif2682KFig. S5. Photocatalytic activity regarding hydrogen production over (Y1.5Bi0.5)1−xTi2O7−3x calcined at 1023 K for 4 h with 0.75 wt% rhodium as co-catalyst in the presence of 10 vol% methanol as sacrificial reagent.
jace12013-sup-0006-FigS6.tifimage/tif2682KFig. S6. Photocatalytic activity regarding hydrogen production over (Y1.5Bi0.5)1−xTi2O7−3x calcined at 1173 K for 4 h with 0.75 wt% rhodium as co-catalyst in the presence of 10 vol% methanol as sacrificial reagent.
jace12013-sup-0007-FigS7.tifimage/tif2682KFig. S7. Photocatalytic activity regarding hydrogen production over (YBi)1−xTi2O7−3x calcined at 1023 K for 4 h with 2.00 wt% platinum as co-catalyst in the presence of 10 vol% methanol as sacrificial reagent.

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