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Figure S1. Reversible photocrosslinking reaction between CNVK and Ψ or U in DNA/RNA heteroduplex.

Figure S2. Predicted structure of DNA/RNA heteroduplexes containing CNVK and Ψ or U.

Figure S3. Ultrahigh performance liquid chromatography analysis of the equimolar mixture of CNVK–ODN and complementary oligoribonucleotide (ORN) containing Ψ or U after the photocrosslinking and photosplitting.

Figure S4. Ultrahigh performance liquid chromatography analysis of the equimolar mixture of CNVK–ODN and complementary ODN containing Ψ, U or T before and after 4 s of photoirradiation.

Figure S5. Time course of the photocrosslinking reaction between CNVK–ODN and complementary ODN containing Ψ, U or T.

Figure S6. HPLC analysis of the degraded product of the two photodimers consisting CNVK–ODN and oligoribonucleotide (ORN) (Ψ).

Figure S7. Temperature dependence of the yield of minor product consisting of CNVK–ODND and ORN(Ψ).

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