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Samuel Bernard, Olivier Majoulet, Fabien Sandra, Annie Malchere and Philippe Miele Direct Synthesis of Periodic Mesoporous SilicoBoron CarboNitride Frameworks via the Nanocasting from Ordered Mesoporous Silica with Boron-Modified Polycarbosilazane Advanced Engineering Materials 15

Article first published online: 19 NOV 2012 | DOI: 10.1002/adem.201200168

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Periodic mesoporous SilicoBoron CarboNitride (Si3.0B1.0C3.9N1.8) frameworks with p6mm hexagonal symmetry, a specific surface area of 337 m2 g−1, a high pore volume (0.55 cm3 g−1) and a narrow pore-size distribution centered on 4.6 nm with an amorphous network remaining stable during continuous heat-treatment to 1400 °C in a nitrogen atmosphere have been prepared by a direct nanocasting process of ordered mesoporous silica with a boron-modified polycarbosilazane (BmPS).

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