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Jia-Hua Ni, Christine J. Frandsen, Li-Han Chen, Yan-Yan Zhang, Jirapon Khamwannah, Guo He, Ting-Ting Tang and Sungho Jin Fabrication of Gradient TiO2 Nanotubes on Ti Foil by Anodization Advanced Engineering Materials 15

Version of Record online: 15 FEB 2013 | DOI: 10.1002/adem.201200311

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Gradient TiO2 nanotubes with tube diameters ranging from 55 to 105 nm and lengths ranging from 300 nm to 500 across 12 mm of Ti foil are obtained by a new anodization based method in HF electrolyte using applied voltage as low as 5–20 V. In the method, the applied anodization voltage is increased step by step, while the Ti foil is immersed into electrolyte progressively during anodization.

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