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Nirmalya Moitra, Kazuyoshi Kanamori, Toyoshi Shimada, Kazuyuki Takeda, Yumi H. Ikuhara, Xiang Gao and Kazuki Nakanishi Synthesis of Hierarchically Porous Hydrogen Silsesquioxane Monoliths and Embedding of Metal Nanoparticles by On-Site Reduction Advanced Functional Materials 23

Version of Record online: 27 DEC 2012 | DOI: 10.1002/adfm.201202558

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Surface-active hierarchically porous monoliths consisting of hydrogen silsesquioxane (HSiO1.5) are prepared via sol-gel accompanied by phase separation. The on-site reduction of aqueous noble metal salts results in the formation and embedding of metal nanoparticles throughout the monoliths. Both the bare monolith and nanoparticle-embedded monolith are promising as reusable and recyclable heterogeneous catalysts.

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