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Jia Hong Pan, Xing Zhu Wang, Qizhao Huang, Chao Shen, Zhen Yu Koh, Qing Wang, Astrid Engel and Detlef W. Bahnemann Large-scale Synthesis of Urchin-like Mesoporous TiO2 Hollow Spheres by Targeted Etching and Their Photoelectrochemical Properties Advanced Functional Materials 24

Version of Record online: 21 AUG 2013 | DOI: 10.1002/adfm.201300946

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Urchin-like mesoporous TiO2 hollow spheres (UMTHS) are successfully prepared on a gram scale by a designed targeted-etching process. The key feature of the strategy is the etching reconstruction of amorphous hydrous TiO2 solid spheres (ATHSS), creating a hollow interior and an urchin-like shell consisting of radially standing single-crystal anatase nanothorns with exposed {101} facets

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