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Beom Jin Kim, Do-Joong Lee, Yang-Rae Kim, Sung Yul Lim, Je Hyun Bae, Ki-Bum Kim and Taek Dong Chung Gold Microshell Tip for In Situ Electrochemical Raman Spectroscopy Advanced Materials 24

Article first published online: 15 DEC 2011 | DOI: 10.1002/adma.201103644

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Tip fabrication by a new strategy is proposed for simultaneous acquisition of electrochemical (EC) signals from an ultramicroelectrode and spectroscopic information from surface-enhanced Raman scattering (SERS). The EC-SERS tip (see figure) is prepared by carefully tuning a SERS-active gold microshell to maximize Raman scattering, mechanically attaching it to the end of a micropipet, and electrically connecting it to a ruthenium inner layer through electroless deposition.

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