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Adham Ahmed, Harald Ritchie, Peter Myers and Haifei Zhang One-Pot Synthesis of Spheres-on-Sphere Silica Particles from a Single Precursor for Fast HPLC with Low Back Pressure Advanced Materials 24

Article first published online: 31 AUG 2012 | DOI: 10.1002/adma.201202810

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Spheres-on-sphere (SOS) silica particles are prepared in a one-pot scalable synthesis from mercaptopropyltrimethoxysilane with hydrophilic polymer and cationic surfactant under alkaline conditions. The SOS particles exhibit solid-core porous-shell properties. The fast separation of small molecules and proteins with low back pressure are demonstrated by high-performance liquid chromatography (HPLC) for the columns packed with SOS-particles.

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