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Yosuke Nakamura, Satoshi Minami, Kazuki Iizuka and Jun Nishimura Preparation of Neutral [60]Fullerene-Based [2]Catenanes and [2]Rotaxanes Bearing an Electron-Deficient Aromatic Diimide Moiety Angewandte Chemie International Edition 42

Version of Record online: 10 JUL 2003 | DOI: 10.1002/anie.200351411

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Crowning glory: An unprecedented [2]catenane that exhibits a donor–acceptor–donor–acceptor stacking motif was obtained through intramolecular Bingel reactions of [60]fullerene monoadducts that bear a naphthalenetetracarboxylic diimide moiety, in the presence of 1,5-dinaphtho[38]crown-10 ether at −78 °C (see scheme; DBU=1,8-diazabicyclo[5.4.0]undec-7-ene).

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