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Emiel de Smit, Ingmar Swart, J. Fredrik Creemer, Chithra Karunakaran, Drew Bertwistle, Henny W. Zandbergen, Frank M. F. de Groot and Bert M. Weckhuysen Nanoscale Chemical Imaging of the Reduction Behavior of a Single Catalyst Particle Angewandte Chemie International Edition 48

Version of Record online: 10 FEB 2009 | DOI: 10.1002/anie.200806003

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A closer look: Investigation of the reduction properties of a single Fischer–Tropsch catalyst particle, using in situ scanning transmission X-ray microscopy with spatial resolution of 35 nm, reveals a heterogeneous distribution of Fe0, Fe2+, and Fe3+ species. Regions of different reduction properties are defined and explained on the basis of local chemical interactions and catalyst morphology.

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