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Dr. Michèle Janssen, Dr. Jos Wilting, Dr. Christian Müller and Prof. Dieter Vogt Continuous Rhodium-Catalyzed Hydroformylation of 1-Octene with Polyhedral Oligomeric Silsesquioxanes (POSS) Enlarged Triphenylphosphine Angewandte Chemie International Edition 49

Article first published online: 8 SEP 2010 | DOI: 10.1002/anie.201001926

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Go with the flow: Homogeneous catalyst recycling can be applied to the production of aldehydes in a continuous flow nanofiltration reactor (see picture) that can operate for an unprecedented period of up to two weeks without showing typical deactivation or leaching phenomena. The catalyst is based on a bulky, rigid, and robust silsesquioxane-modified PPh3 ligand, and combines efficient recovery with high activity and selectivity.

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